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VIP会员企业 一种纳米级防水微粉产品及其制备方法
对应类别: 化工、石油、冶金     所属地区:北京市 → 朝阳区
申请类别:发明专利 授权日期:2014-1-25
专 利 号:ZL02157969.5 专利权人:闫新育 洪重光
合作方式:专利权转让, 区域独占, 普通许可, 面议
电    话:13021253375
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邮政编码:100029 要发平信,不适于接收挂号信
电子信箱:yanliuxinyu@sohu.com
联系地址:北京市朝阳区德胜门外祁家豁子华严北里9号楼1门1501号
网站地址:http://
项目介绍:

 

    1、基本原理(产品制备及应用): 产品制备原理工艺路线及应用: 在第一密闭反应斧中用甲基卤硅烷与水反应制备甲基硅酸;再在第二反应釜中将饱和烧碱溶液在加热及搅拌下加入定量甲基硅酸;在第三反应釜中在较低温度下用酸溶液慢反应至规定酸度下反应完毕;将制品尽可能滤去水分成近似豆腐渣状;用分散干燥机(即有分散功能又有瞬间干燥功能)制备成干燥纳米级微粉。

    本工艺主要创新点在于将普通粗颗粒防水作用不大的甲基硅酸再加工,制备成纳米级超细微粉聚甲基硅酸。原品颗粒度仅在几百微米左右,而新产品却达到了一点几个纳米,颗粒度降低数万倍以上。由此使在防水应用领域有跨时代意义。如水泥颗粒克比表面积为300平方米左右,纳米粉则提高数千倍。例如,二克纳米粉加入到一公斤水泥中搅匀后,纳米粉可完全覆盖包裹住水泥颗粒,经标准水泥物理检验方法制备,经28天养护期后,测得抗压抗折强度与空白值对比都有达提高水泥一个标号(这是由于纳米粉对水泥颗粒包裹形成直径为100200纳米的团粒结构体,使新结构具有排列有序均匀及达到纳米级间隔的致密程度。由此混凝土致密度明显提高了,表观没有孔洞及微孔。由此在抗渗,抗酸,耐久及由于提高水泥标号而提高水泥厂经济效益方面可大有作为。

    纳米防水粉除应用在制备防水水泥外也可用于防水建材制备及提高某些防水涂料的防水性。建材如制备防水腻子等等。

    对于水泥厂而言,可以自生产纳米粉,除保证自用之外还可外销,会得广销门路而获好的经济效益。

    2、投资效益及应用前景分析: 在有厂房,库房及场地条件下,投资二、三佰万元用于生产设备,原料等流动资金,人员工资。在生产设备购到后在一年内可出产品。按内用算200万吨水泥厂全加入钠米粉(0.2%),需要生产纳米粉4000吨,如按加一半算可用2000吨,其余可外销。究竟产销多少可视销售实情而定。就以年产4000千吨纳米粉计算,原料价格4000/吨左右,纳米粉生产成本按2000/吨算,按产品1.0万元使用价值(可理解为销售价格)算,加入水泥重量的0.2%,纳米粉成本则为12/吨水泥,实际可加入0.15%,则为9元。如按提高水泥一个标号20元多销售额算,可净得10/吨以上。而且作为制备抗渗、抗酸及高密度、更耐久性混凝土的特种水泥,销售价格可以更高,因而更具有使用价值和应用前景。

    3、关于工艺产生不产生污染物问题: 本制备工艺产出的副产品没有环境污染,属于无机盐类,没有气味不污染空气和水源及土壤。副产物经干燥后是一种无机化工原料,又可销售获得一定经济效益。

    4、本中国发明专利不属于企业公司。专利证书扫描件另附。

    5、合作意向及联系方式: 本人希望采用技术转让方式,可按区域垄断(区域范围指以省划界,或东南西北区域划分,如东北,华中,东南,西北,华南,西南等),不是全国独家垄断是因为水泥厂高使用量纳米粉,只一个生产厂生产纳米粉不可能量太大,所以适当分散生产是必要的,以保证更多纳米粉产出使应用量能更多。 无论那种交易方式都是面对大企业。如是技术入股,要有预付入门费要求。

 

  1, the basic principle of preparation and application of (product) : the principle of preparation of process route and application of products: in the first closed reaction axe reaction with methyl halide silane and water preparation of methyl silicate; And then in the second reaction kettle will be saturated in caustic soda solution under the heat and stir add quantitative methyl silicate; At lower temperatures in the reaction kettle 3 slow reaction with acid solution to the regulation of acidity of reaction is completed; Products filter the water as much as possible into the approximate shape of bean curd; With scattered drying machine (i.e., have the functions of decentralized and instant dry) preparation of nanoscale powder into dry.

   This process main innovation point is that the ordinary coarse particle waterproof does little methyl silicate reprocessing, poly (methyl silicate into the nanoscale ultrafine powder preparation. The original product granularity in only a few hundred microns, and the new product is to achieve a bit of a few nanometers, reducing the particle size, more than tens of thousands of times. The resulting in waterproof application fields a cross time significance. Particles, such as cement specific surface area is about 300 square meters, the nano powder is thousands of times. , for example, 2 grams of nanometer powder to stir in one kilogram of cement, wrapped in nanometer powder can be completely cover cement particles, the preparation of standard cement physical test methods, after 28 days curing period, measured compressive flexural strength improving compared with blank value of cement a label (this is due to the nanometer powder of cement particles wrapped to form a diameter of 100-200 - nanometer granule structure, make the new structure has an orderly uniform and dense degree of reach nanoscale interval. The concrete density significantly increased, apparent without holes and micro hole. Thus in impermeability, resistance to acid, durable and due to improve the cement mark can go a long way in improving economic efficiency of cement plant.

   Nano waterproof powder in addition to the application in the preparation of waterproof cement can also be used for the waterproof building materials preparation and improve the water proofing property of some waterproof coating. Building materials such as preparation of waterproof putty and so on.

For cement plant, can from the production of nanometer powder, in addition to guarantee for private use can also export, get well-sold access and obtaining good economic benefits.

  2, the investment benefit and the application prospect of analysis: in workshop, warehouse and site conditions, 2, 3 usd $ten thousand for the production of equipment, raw materials such as liquidity, personnel salary. Within a year after production equipment bought the product. According to use 2 million tons of cement in the adding sodium rice (0.2%), needs to produce nano powder 4000 tons, such as calculate by add half 2000 tons are available, and the rest can be exported. How many visual production sales of the truth. Calculated with annual output of 4 million tons of nanometer powder, raw material price 4000 yuan/tons, nanometer powder production cost calculate by 2000 yuan/ton, 10000 yuan price for the products use value (can be understood as a sales price), add 0.2% by weight of the cement, the nano powder cost for 12 yuan/tons of cement, can be added to 0.15% in real terms, is 9 yuan. As a label by improving cement sales more than 20 yuan, could net 10 yuan/tons. And as a preparation impermeability, resistance to acid and high density, the durability of concrete special cement, sales prices are higher, and therefore has more use value and application prospect.

  3, about the process does not produce pollutant problems: the preparation technology of output a by-product of no environmental pollution, belonging to inorganic salts, no odor polluting the air and water and soil. By-products after drying is a kind of inorganic chemical raw materials, but also sales to obtain certain economic benefits.

  4, this Chinese invention patent does not belong to the company. Patent certificate scanned documents attached.

  5, cooperation intention and contact way: I want to use the technology transfer way, according to the regional monopoly (area to save demarcation, or with the southeast of the northwest division, such as the northeast, central China, southeast, northwest, south China, southwest, etc.), is not the exclusive monopoly because of high cement plants use nanometer powder, not only a factory production of nanometer powder energy is too big, so it is necessary to properly diversified production, to ensure more nanometer powder are more output. No matter that kind of way to trade is faced with big companies. So technology investment, want to have a prepaid fee.

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